| Product |
5-Bromo-4-chloro-3-indolyl
b-D-glucuronide cyclohexylamine salt (X-Gluc) |
| Molecular
Formula |
C20H26BrClN2O7 |
| Molecular
Weight |
521.80 |
| CAS No. |
18656-96-7 |
| Appearance |
Crystalline
white powder. |
| Melting Point |
Slow
colorization > 140 °C. Gave no clear melting point. |
| Solution |
Clear solution
when dissolved in DMF (5mg/ml). |
| Purity |
> 98%
by TLC and NMR. |
| Thin Layer
Chromatogram (TLC) |
Single spot.
Solvent: Chloroform : MeOH : H2O = 65 : 35 : 8
Detection: - UV 254 nm
- 10% H2SO4
in EtOH and heat
- Silica gel 60
(Machery-Nagel, Alugram Sil G/UV254)
|
| - 300 MHz 1H-NMR
in D2O |
Conform with the
structure. |
| Storage |
Store at 4 ° C and protect from light and moisture. |
| Remarks |
Toxicity
unknown. Avoid exposure.
Preparation of solution just prior to use is recommended.
UV-spectroscopic grade of DMF is recommended when preparing the DMF solution. |
Carbohydrates
